DSC PT 1600
High temperature Differential Scanning Calorimeter (HDSC) up to 1750°C
Differential Scanning Calorimetry (DSC) is the most common thermal analysis method due to its wide range of information provided. The LINSEIS high temperature DSC PT 1600 (HDSC/DTA) is designed to deliver highest calorimetric sensitivity, short time constants and a condensation free sample chamber.
These features guarantee superior resolution and baseline stability over the entire instrument lifetime. This provides an indispensable tool for material development, R&D and quality control.
The modular concept of the HDSC and DTA systems allows the use of different furnaces with a temperature range from -150°C up to 1750°C.
The vacuum tight design enables quantitative enthalpy and Cp (Specific Heat) determination under the cleanest atmospheres and under vacuum of 10E-5mbar. The systems can be upgraded with an optional sample robot and coupled to a MS or FTIR.
User friendly exchangeable measureing systems such as a DTA Sensor and two different DSC Sensors are available. Each DSC Sensor is available as type E, K, S, B for the DSC PT 1600.
This allows the perfect chioce for any application, temperature or atmosphere.
|Model||DSC PT 1600*|
|Temperature range:||-150°C up to 700°C, RT up to 1600/1750°C|
|Sensor Types:||DTA / DSC / DSC – Cp|
|Heating rates:||0.001 K/min … 50 K/min|
|Cooling rates**:||0.001 K/min … 50 K/min|
|Measuring range:||0.1 up to 4000 W/(m∙K)|
|Atmospheres:||reducing, oxid., inert (static, dynamic)|
*Specs depend on configurations
** temperature dependent
All thermo analytical devices of LINSEIS are PC controlled and the individual software modules exclusively run under Microsoft Windows operating systems. The complete software consists of 3 modules: temperature control, data acquisition and data evaluation.
The Linseis 32 – bit software encounters all essential features for measurement preparation, execution and evaluation with a DSC run, just like with other thermo analytical experiments. Due to our specialists and application experts LINSEIS was able to develop this easy understandable and highly practical software.
- Temperature Modulated DSC
- Repetition measurements with minimum parameter input
- Evaluation of current measurement
- Curve comparison up to 32 curves
- Curve subtraction
- Multi-methods analysis (DSC TG, TMA, DIL, etc.)
- Zoom function
- 1. and 2. Derivative
- Multiple smoothing functions
- Complex peak evaluation
- Multipoint calibration for sample temperature
- Multipoint calibration for change of enthalpy
- Cp calibration for heat flow
- Storage and export of evaluations
- Program capable of text editing
- Export and import of data ASCII
- Data export to MS Excel
- Signal-steered measuring procedures
- Zoom in function
- Undo function
Applications example: Ferrite’s production
The components used for production of magnetic ferrite’s are ZnO, Fe2O3 and Cr2O3. Cr2O3 is added for modifications of the magnetic and electric properties. At 735°C the powder forms a mixed ferrite with a signal structure (exothermic reaction: -20.6 J/g).
Above 1034°C and 1321°C the heat flow deviates strongly into the endothermic direction due to melting of different phases. The Linseis DSC PT1600 with the type S-measuring head provides a very stable baseline with an extremely low noise level up to 1450°C. This high sensitivity is essential to perform exact enthalpy measurements and evaluations.