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GSA PT 1000

High End Pressure Sorption Measurements

Description

On point

Linseis offers a wide range of Gravimetric Sorption Analyzers. Our integrated solution offers the ability to independently software control the pressure, temperature and gas dosing. Our GSA PT 1000 line is based on the well proven linseis microbalance design. This ultra sensitive microbalance is available in two version 0,1 / 1 ug for 5 / 25 g sample weight.

A number of environmental chambers are available for operations from -150 up to 1800°C and UHV (ultra high vacuum) to 350 bar. An optional TG-DSC Thermogravimetry – Differential Scanning Calorimetry measuring head allows the simultaneous determination of weight change and caloric reactions in one run. Optional gas and vapor dosing systems as well as residual gas analysis is available.

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Specifications

Black and white
Model GSA PT 1000 HP 1
Temperature range:  RT up to 1100°C
Max. pressure: max. 150 bar
Vacuum: 10E-4 mbar
TGA
Max. sample mass: 2/15/100g
Resolution: 0.1/0.5/10 µg
DSC
DSC resolution: 0.3/0.4/1 µW
DSC sensors: E, K, S, C
DTA:
DTA sensitivity: undefined
Options: Pressure controlable Gas Mixing System (MFC´s)
Atmosphere: inert, oxid.*, red., vak. 

* not possible with Graphite heater

Model GSA PT 1000 HP2
Temperature range: RT up to 1400/1800°C
Max. pressure: max. 50 bar
Vacuum: 10E-4 mbar
TGA
Max. sample mass: 2/15/100g
Resolution: 0.1/0.5/10 µg
DSC
DSC resolution: 0.3/0.4/1 µW
DSC sensors: E, K, S, C
DTA:
DTA sensitivity: undefined
Options: Pressure controlable Gas Mixing System (MFC´s)
Atmosphere: inert, oxid.*, red., vak. 

* not possible with Graphite heater

Software

All LINSEIS thermo analytical instruments are PC controlled. The individual software modules exclusively run under Microsoft® Windows® operating systems. The complete software consists of 3 modules: temperature control, data acquisition and data evaluation. The 32 bit software incorporates all essential features for measurement preparation, execution, and evaluation of a STA measurement. Thanks to our specialists and application experts, LINSEIS was able to develop comprehensive easy to understand user friendly application software.

TG – Features

  • Mass change as % and mg
  • Rate Controlled Mass Loss
  • Evaluation of mass loss
  • Residue mass evaluation

General Features

  • Program capable of text editing
  • Data security in case of power failure
  • Thermocouple break protection
  • Repetition measurements with minimum parameter input
  • Evaluation of current measurement
  • Curve comparison up to 32 curves
  • Storage and export of evaluations
  • Export and import of data ASCII
  • Data export to MS Excel
  • Multi-methods analysis (DSC TG, TMA, DIL, etc.)
  • Zoom function
  • 1 and 2 derivation
  • Programmable gas control
  • Statistical evaluation package
  • Free scaling

Applications

  • Gas Sorption Analysis
  • Sorption Enthalpies (Simultaneous TG/DSC-Sensor)
  • Density Determination
  • Gas Storage
  • Zeolites
  • Catalysts
  • In-situ Gas Analysis (FTIR, Raman, ELIF)
  • Kinetic Analysis
  • Corrosive Atmospheres – Magnetic Suspension Balance
  • Adsorption Isotherms (BET Surface Analysis)
  • TPD, TPO, TPR measurements (-196 to 1800 °C)
Anwendungsbeispiel: TPD, TPO and TPR measurements:

The distribution and relative strength of acid sites in zeolithes are important indicators of its catalytic properties. The acidity of zeolithes can be accurately measured with the temperature programmed desorption (TPD) of a base from the zeolithe surface. The Linseis gravimetric Sorption Analyzers are useful tools for characterizing TPD, TPO or TPR profiles.

The figure below shows the chemidesorption of ammonia from a zeolithe catalyst surface. Weakly bound ammonia molecules are desorped between 100 and 250 °C. Between 260 and 500 °C strongly bound ammonia is desorped. The amounts of desorped ammonia can be quantitatively measured, i.e. it is possible to quantitatively identify the number of strong and weak acid sites present in the sample.

GSA Applikation TPD-, TPO- and TPR-Messungen

Anwendungsbeispiel: In-Situ-FTIR

In-situ FTIR measurement during CO2 gasification of an anthracite in a TGA system (sample temperature: 1100°C, pure CO2 atmosphere [gas flow rate: 20 ml/min at 273 K, 0.013 bar] during FTIR measurement, FTIR measurement: 30 s, CO absorption at 4300 cm-1, CO2 absorption at 4900 cm-1)

GSA In-Situ-FTIR Applikation

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Overview

Linseis Produktbroschüre GSA

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