TMA PT 1600
Vertical Thermomechanical Analyzer TMA PT1600
Description
On point
The design of the TMA PT 1600 Thermomechanical Analyzer guarantees highest precision, reproducibility and accuracy. The system was constructed to performing a variety of Thermomechanical experiments, on an array of sample shapes and sizes, over a wide temperature range, to meet all TMA needs. The system can perform either static or dynamic measurements due to a built in force/frequency generator.
Typical materials under investigation are: composite materials, glass, polymers, ceramics and metals. The variety of measuring systems allows sample geometries such as fibers, rods, films, rods or cylinders.
TMA / DTMA Features
With low constant load:
- Linear thermal expansion evaluation
- Change of volume
- Phase transformation
- Sinter process evaluation
- Softening point determination
- Transformation points
- Swelling behavior
- Tension
With increased constant load:
- Penetration
- Transition and comparison tests
- 3 point bending test
With dynamic load:
- Visco-elastic behavior
Additional optional features:
- DTA evaluation
- (RCS) Rate controlled sintering software
Specifications
Model | TMA PT 1600 |
---|---|
Temperature range: | RT up to 1600°C |
Price range: | $$ |
Sample size: | 30 mm |
Force: | up to 1/5.7/20 N |
Frequency: | 1 Hz |
Resolution: | 0.125 nm |
Atmospheres: | red., inert, oxid., vac. static/dynamic |
Electronics: | Integrated |
Interface: | USB |
Accessories
- Liquid nitrogen cooling accessory (automatic control of LN2 supply)
- Turntable for multiple furnace configuration
- Selection of fused silica / stainless steel sample holders and probes of various geometries
- Vernier caliper for online input of the sample length
- Selection of vacuum and turbo molecular pumps
- Manual, semi-automatic and automatic (MFC) gas control boxes
Software
All LINSEIS thermo analytical instruments are PC controlled. The individual software modules exclusively run under Microsoft® Windows® operating systems. The complete software consists of 3 modules: temperature control, data acquisition and data evaluation. The 32 bit software incorporates all essential features for measurement preparation, execution, and evaluation of a Thermogravimetric measurement. Thanks to our specialists and application experts, LINSEIS was able to develop comprehensive easy to understand user friendly application software.
TMA-Features
- Glass transition and softening point evaluation
- Softening point detection with automatic software controlled system shut down
- Display of relative/absolute shrinkage or expansion curves
- Presentation and calculation of technical / physical expansion coefficient
- Rate Controlled Sintering (RCS) Software
- Sinter process evaluation
- Semiautomatic evaluation functions
- Several system correction features
- Automatic zero point adjustment
- Automatic software controlled sample pressure adjustment
General Features
- Program capable of text editing
- Data security in case of power failure
- Thermocouple break protection
- Repetition measurements with minimum parameter input
- Evaluation of current measurement
- Curve comparison up to 32 curves
- Storage and export of evaluations
- Export and import of data ASCII
- Data export to MS Excel
- Multi-methods analysis (DSC TG, TMA, DIL, etc.)
- Zoom function
- 1 and 2 derivation
- Programmable gas control
- Statistical evaluation package
- Free scaling
Applications
Application example: Elastomer (non high temperature in this case)
Because of their very special and versatile properties, polyurethanes Elastomers have found wide application in virtually every industry, varying from the automotive, electrical and electronic industry, design and textile industry, to the mining and heavy duty industry.
Evaluation of Elastomers specifically developed for applications above 0°C. The glass point was detected at 29.9°C. When further increasing the temperature, additional expansion of the material in the elastic range occurs. The plastic range of the material has not been reached during this evaluation.
External application:
Preparation of rigid polyurethane foams as inner wetted thermal insulation (published AIP Conference Proceedings)
Rigid Polyurethane Foams as External Tank Cryogenic Insulation for Space Launchers (published IOP Conference Series: Materials Science and Engineering)